Continuous Flow Reactor Optimization
Reduced residence time variation by 15%Objective
Transition a batch synthesis process to a continuous flow reactor to improve throughput.
Approach
Modeled kinetics in Python to determine optimal tubing diameter and length. Implemented static mixers to improve heat transfer coefficients.
Result
Achieved steady state in 12 minutes with a 15% reduction in residence time variance. Yield increased by 4% due to better thermal control.
Pump limitations required ΔP < 4 bar.
Investigate inline IR spectroscopy for real-time QC.